Uses:

Jacketed glass reactor design for the double-glazed inner layer into the the reaction menstruum do stirring reaction, sandwich can pass on a variety of hot and cold sources (frozen liquid, hot water or hot oil) do loop heating or cooling reaction. Can be used according to requirements set isothermally in a sealed glass reactor, under conditions of atmospheric pressure or negative pressure, the reaction was stirred and refluxed with distillation of the reaction solution is do the modern Fine Chemical, biopharmaceutical test, production equipment and the ideal synthesis of new materials.

 Our company's Jacketed glass reactor set domestic advantages of similar products, positive customer suggestions and experience, has formed a 1L, 2L, 3L, 5L, 10L, 20L, 30L, 50L, 80L, 100L Series.

Features：

1. Using Teflon composite seal, can maintain a high degree of vacuum.

2. Efficent condenser to ensure high recovery.

3. The full set of glass GG3.3 high borosilicate glass production, good chemical and physical performance.

4. Hot oil on glass interlayer interface pass through the loop, to do the reaction in the high temperature state; pass on the cooling liquid can be carried out under a low temperature state reaction. It also can connect tap water to let heat away rapidly.

5. The decentralization material flange mouth and the PTFE valve, container no dead ends, removable to facilitate the discharge of solid materials.

6. Stirring motor digital frequency conversion control, supporting increased torque reducer.

7. Reasonable structure, and material stresses. Mechanical parts made of stainless steel and aluminum parts.

The glass pieces used in all high-temperature and high chemical properties of borosilicate glass. Electrical components parts: the main components imported raw devices.

I、Installation

Jacketed glass reactor framework part of the glass part of securing clamps part, stirring part of the four major components, easy installation.The specific procedures are as follows:

1、 Stainless steel frame assembly in accordance with the standard framework Do not chucking any internal hexagonal stainless steel screws.

2、 Adjust the low position of the stainless steel frame to the actual ground leveling as standard, the card tight all stable hexagonal screws.

3、 The locking framework at the bottom of the pulley, the installation of the reactor body, this action requires two people at the same time coordinating completed, adjust the the reactor body horizontal and vertical position.

4、 Blender motor parts, do not card a tight hexagonal screws.

5、 Stir sealing plugs and stirring rod, spin out of tetrafluoroethylene card cap, the fixed stirring sealing plug in the cover flange stirring port.

6、 The of retrofitting fixed kettle cover cards enhance stirring rod depth motor stirring gimbal trumpet hexagonal stainless steel tool clamping hexagonal stainless steel screws.

7、 Overall screws and cards all fixed tight, the installation of the condenser and constant pressure funnel stainless steel support bar.

8、 Reflux condensation elbow cards installed in the kettle cover the installation of the return pipe installation of the condenser. Constant pressure funnel cover the installation in the kettle, the installation of thermowells and installation of glass bleed valve.

9、 Digital converter installation location, this time installed.

II、Usage 1、Check the power supply voltage and machine nameplate specifications.

2、Plug in the power cord, open the power switch on the inverter speed control knob to select the appropriate speed (at the same time in the

display window shows speed).

3、The flow of materials and the power of the motor speed may at some point have a resonance, due to changing the motor speed to avoid resonance.

4、Stirring rod fitted must be rotated by hand, pay attention to concentricity (verticality), as the heart of a (vertical) bad should loosen heavy

folder, the folder is then open power gradually adjust from slow to fast.

5、Stirring rod adjustable wrenches, according to need so that the stirring rod moves up and down, the maximum moving distance is 50mm.

6、Found the reactor sealing performance decline, please check stirring the tetrafluoroethylene between the rod and the lid of the reactor

sealing plug.

7、The reactor glass pieces all GG3.3 low coefficient of expansion and high temperature quality borosilicate glass manufacturing, glass can withstand the highest temperature: 280 ℃, bear minimum temperature: -80°C.

8、Glass reactor imports and exports pass on the hot oil do heating reaction, coolant can pass on the low-temperature reaction, if the use of

steam-heated, not more than 0.5K-1K. (Note: Do not try to take advantage of the pressure steam heating).

9、 When the test is carried out at low temperatures, the discharge valve at the bottom of frosting, use this valve must first partial thaw before

using to prevent the minced glass.

10、Materials of the reactor are subject to particles, discharge may be remaining in the the polytetrafluoroethylene piston valves to be used

again when the airtightness is influential. Be sure each discharge cleaning of clean and re-use.

12、The reactor was heated using a high-temperature cycle heating operation, cooling should be used a low-temperature circulator performs

the cooling operation.

13、Before the use of the reactor was added to the reaction material, and then heating or cooling. Avoid reactor materials, heating or cooling in

the mezzanine.

14、Reactor requires heating or cooling, should adopt high temperature circulator or cryogenic circulator heating cycle or cycle cooling, should

first heat recirculation or before refrigeration recycling.

15、Reactor under high temperature needed cooling, heating switch first turn off the high-temperature cycle (cycle switch remains open), adding water or oil, and in circulation within the temperature gradually cooling. Drained reactor mezzanine avoid heating the material, direct

cooling loop new substances.

III、Safety Precautions

1、All glass pieces to be cleaned before installation.

2、Each standard port, milling mouth and sealing surfaces to be coated with a small amount of vacuum grease, increase the air tightness.

3、Before the installation, use, maintenance, inspection, be sure to familiarize themselves with the entire contents of the manual to use it right.

4、The supply voltage must be consistent with the provisions of this instrument.

5、No-load should not be high-speed operation.

6、The life of the electrical box and the ambient temperature, humidity. Please keep the governor and the motor dry.

7、Install the equipment of the reactor operation by professional operators using the device.

8、 5 minutes off the power, do not touch the electrical parts, may still be due to the inverter or capacitor discharge electric shock.

9、 Operation, pay attention to the the body hard objects (watches, rings, belt buckles, etc.) of glass crashing damages.

10、Connected vacuum tube pipe when we must be careful to avoid excessive force on the broken glass on the human body injury.

11、 High temperature cycle oil bath, pay attention to the damage of the high temperature of the human body, I recommend

using a small damage to the human body's heat-conducting oil as a solvent (dimethyl silicone oil, a viscosity of 100 or 50). In particular, pay attention to the high-temperature cycle, should be open circulation pump, the thermal conductivity solvent cycle, gradually warming.

12、Installation is complete wheel locking bracket, to avoid moving.

13、Vacuum grease on the glass cock or feeding tube rotatable parts, please use silky and viscous materials.

14、Please send Gentle vacuum grease evenly thin smear on the spool, to cooperate fully with the grinding mouth.

15、Grinding mouth parts daub vacuum grease, after a long period of use, the grease will oxidize or harden, resulting in

grinding mouth parts of the rotation difficult or sticky death. Therefore, before the grease hardens, periodically removing the component with a paper towel to wipe the grease above, and then carefully wipe clean with solvents such as toluene and xylene. To be complete evaporation of solvent, re-to smear new vacuum grease.

16、Grinding mouth fastened or glued dead, then force it demolition caused by broken glass, very dangerous. Grinding mouth sticky death phenomenon, vacuum grease softening after removal methods (hot water, heating torch) curing.

(If the cement is very serious, forced removal is very dangerous. Encounter this situation, please contact the company's after-sales service department.)

About motor temperature rise:

This instrument motor with class E insulation, polyester high strength enameled wire winding, the use of the environment, an altitude of over 1000 meters, the ambient temperature does not exceed 40 ° C continuous use motor surface temperaturerise (the difference between the motor surface temperature and ambient temperature does not exceed 90 ° Cis normal and can be freely used). Temperature exceeds 90 ° C. To check the relevant transmission lubrication system, if the ambient temperature is high, the user can use the fan cooling.Caution must be strictly observed, or may cause injury to personnel or damage to the machine.

IV、Maintenance Instructions

1、Carefully before checking instruments, glass bottles if there is damage, the interface is consistent attention to gently.

2、With a soft cloth (available napkins alternative) wipe each interface, and then smear a little vacuum grease. (With vacuum grease must be covered to prevent gray sand to enter.)

3、Each interface can not be screwed too tightly to regularly loose, to avoid long-term furrowed lead connector killed.

4、First open the power switch, and then let the machine operation from slow to fast, stop to wait for the machine in the stopped state, the off switch.

5、Throughout polyfluo switch can not tighten too hard, easy to damage the glass.

6、After each use with a soft cloth to wipe remain at the surface of the machine traces of oil, stains, solvents remaining kept clean.

7、After the shutdown Loosen each PTFE switch, make long-term stationary work state PTFE piston deformation.

8、Of the seals on a regular basis to clean: remove the seals, check the shaft accumulate dirt, wipe with a soft cloth, and then coated with a little vacuum grease, re-fitted to keep the shaft and seals smooth.

9、The electrical part of the water is not available, non-damp.

10、Must purchase original authentic accessories, free to use other accessories of the machines will cause damage.

11、Do any repair or inspection of the machine, be sure to cut off power and water supply.

Notice: The glass pieces is a fragile product, users Handle with care when in use, the damage to the fragile is not within the scope of the company's warranty, if the customer needs, our company will be charged the cost.

V、Fault Simple Exclusion